The textbook was developed in accordance with the requirements of the third generation of the Federal State Educational Standard of Higher Professional Education and the work programs of KNRTU in the disciplines "Analytical Chemistry and FHMA", "Analytical Chemistry" and "Physical and Chemical Analysis". The textbook has a production orientation and contains sections on the analytical control of production, the organization of the work of the analytical service at enterprises, and the features of the analysis of profile groups of objects. At the same time, a significant place in it is given to familiarization with the fundamental foundations of science, a description of the principles that determine various physicochemical and physical methods of analysis. The textbook meets the modern content of analytical chemistry, science and practice of analytical services.